Determination of 3-MCPD in Some Edible Oils using GC-MS/MS
نویسندگان
چکیده
The presence of 3-monochloropropanediol (3-MCPD) in edible oils has been widely reported with its potential health risks. aim this study was to apply optimized recent updated and validated enhanced swift analytical indirect method for determining 3-MCPD consumed (palm, palm olein, extra virgin olive, corn, sunflower, soybean, olive pomace) blend 5% sunflower oil oil, using selective sensitive gas chromatography tandem triple quadrupole mass spectrometry (GC-MS/MS) employing deuterated (3-MCPD-d5) as internal standard (IS) during the entire procedure obtain precise accurate results. occurrence variation contents among studied were found different levels ranged from 93.1 µg/kg 5634.1 samples, maximum value assigned (5634.1 µg/kg) followed by olein (5576.8 µg/kg), corn (2447 (1817.3 soybean (1486.1 pomace (572.5 (210 (93.1 µg/kg). Palm, out limits recommended Commission Regulation (EU) 2020/1322, whereas, compliance within EU. Moreover, content could be used a good tool authenticity quality genuine oil.
منابع مشابه
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ژورنال
عنوان ژورنال: Egyptian Journal of Chemistry
سال: 2021
ISSN: ['0449-2285', '2357-0245']
DOI: https://doi.org/10.21608/ejchem.2021.64084.3373